반응 #215186

반응 방정식

1-Allyloxy-3-phenyl-7-nitro-naphthalene

decaline

→

2-Allyl-3-phenyl-7-nitro-1-naphthol

반응 조건

후처리

1. 1
   온도maintained under nitrogen
2. 2
   온도After cooling
3. 3
   기타the crystals formed
4. 4
   세척were washed with petroleum ether
5. 5
   여과filtered off
6. 6
   기타dried at 80° C. under reduced pressure

실험 절차

31 g of 1-Allyloxy-3-phenyl-7-nitro-naphthalene prepared in step (3) were gradually heated to 180° C. in 390 ml of decaline, the solution being stirred and maintained under nitrogen. The temperature of 180° C. was maintained for about 1 hour. After cooling, the crystals formed were washed with petroleum ether, filtered off and dried at 80° C. under reduced pressure.

출처