반응 #2151

ord-42707e6a793c47a1b88ab3c47a28095a

반응 방정식

CCCCn1cnc2c1c(=O)[nH]c(=O)n2CCCC
3,7-dibutyl-xanthine
CP(C)(=O)CCl
chloromethyldimethylphosphine oxide
→
CCCCn1cnc2c1c(=O)n(CP(C)(C)=O)c(=O)n2CCCC
[1-(3,7-Dibutylxanthin-1-yl)methyl]dimethylphosphine Oxide

반응물

CCCCn1cnc2c1c(=O)[nH]c(=O)n2CCCC
3,7-dibutyl-xanthine
CP(C)(=O)CCl
chloromethyldimethylphosphine oxide

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The title substance was prepared from 5 g (0.0189 mol) of 3,7-dibutyl-xanthine and 2.9 g (0.0227 mol) of chloromethyldimethylphosphine oxide analogously to Example 67.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05728686uspto-grants-1998_03