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4-(6-piperidinohexyl)-3,5-dioxomorpholine p-toluenesulfonate

p-toluenesulfonate

sodium hydroxide

4-(6-piperidinohexyl)-3,5-dioxomorpholine

→

sodium [2-(6-piperidinohexyl)amino-2-oxoethoxy]acetate

sodium tosylate

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실험 절차

Preparation in situ from 4-(6-piperidinohexyl)-3,5-dioxomorpholine-p-toluenesulfonate. 43 milligrams (0.095 millimole) of 4-(6-piperidinohexyl)-3,5-dioxomorpholine.p-toluenesulfonate (prepared as described in Example IX) was dissolved in 2 milliliters of 0.1 N sodium hydroxide (0.2 millimole) to obtain an aqueous solution of sodium [2-(6-piperidinohexyl)amino-2-oxoethoxy]acetate and sodium tosylate. The solution had the following spectral characteristics:

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