반응 #2146061

반응 방정식

N-(4-methylphenyl)-N-benzylamine

isopropyl phosphonic dichloride

→

1-isopropyl-2-(4-methylphenyl)-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide

수율 32.0%

반응 조건

실험 절차

The procedure of Example 1 was employed utilizing N-(4-methylphenyl)-N-benzylamine and isopropyl phosphonic dichloride to yield 1-isopropyl-2-(4-methylphenyl)-2,3-dihydro-1H-2,1-benzazaphosphole-1-oxide (5.4 g, 32% yield) as white crystals having a melting point of 135°-137° C. and the following analysis:

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