반응 #214424

ord-828bbc97c0e948c6a7636eca3a9ec487

반응 방정식

CC(C)(CCl)C(=O)C(Oc1ccc(-c2ccc(Cl)cc2)cc1)n1ccnc1.O=S(=O)(O)c1cccc2c(S(=O)(=O)O)cccc12
4-chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1-(imidazol-1-yl)-butan-2-one naphthalene-1,5-disulphonate
O=C([O-])O.[Na+]
sodium bicarbonate
→
CC(C)(CCl)C(=O)C(Oc1ccc(-c2ccc(Cl)cc2)cc1)n1ccnc1
4-Chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1-(imidazol-1yl)-butan-2-one

반응물

CC(C)(CCl)C(=O)C(Oc1ccc(-c2ccc(Cl)cc2)cc1)n1ccnc1.O=S(=O)(O)c1cccc2c(S(=O)(=O)O)cccc12
4-chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1-(imidazol-1-yl)-butan-2-one naphthalene-1,5-disulphonate
O=C([O-])O.[Na+]
sodium bicarbonate

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

The 4-chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1-(imidazol-1-yl)-butan-2-one naphthalene-1,5-disulphonate obtained according to Example 4 was neutralized with sodium bicarbonate solution. 4-Chloro-1-[4-(4-chlorophenyl)-phenoxy]-3,3-dimethyl-1-(imidazol-1yl)-butan-2-one of melting point 97°-99° C. was obtained quantitatively.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04255434uspto-grants-1981_03