반응 #214414

ord-2671af9b7987409691ffd6a99bf7c164

반응 방정식

CCC1(C)SC(=NO)N=C1C
2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-oxime
CC(=O)N(C)C(=O)Cl
N-acetyl-N-methyl-carbamoyl chloride
→
CCC1(C)SC(=NOC(=O)N(C)C(C)=O)N=C1C
2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-O-[methyl(acetyl)carbamoyl]oxime

반응물

CCC1(C)SC(=NO)N=C1C
2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-oxime
CC(=O)N(C)C(=O)Cl
N-acetyl-N-methyl-carbamoyl chloride

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-oxime was reacted with N-acetyl-N-methyl-carbamoyl chloride as described above to yield 2-oxo-4,5-dimethyl-5-ethyl-3-thiazoline-O-[methyl(acetyl)carbamoyl]oxime, m.p. 98°-101° C.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04255436uspto-grants-1981_03