반응 #214015

반응 방정식

2-chloromethyl-2-imidazoline hydrochloride

2,3-dimethylaniline

→

final product

수율 77.0%

2-(2',3'-Dimethylphenylaminomethyl)-2-imidazoline hydrochloride

수율 77.0%

용매

ethanol

반응 조건

후처리

1. 1
   온도After cooling
2. 2
   기타the crystallised substance is collected by suction
3. 3
   기타recrystallised from water

실험 절차

31 g of 2-chloromethyl-2-imidazoline hydrochloride and 48.4 g of 2,3-dimethylaniline are refluxed for 5 hours in 65 ml of absolute ethanol. After cooling, the crystallised substance is collected by suction and recrystallised from water, affording 36 g (77% yield) of the final product with a melting point of 242° C.

출처