반응 #2139935

반응 방정식

t-butylacrylate

acrylic acid

2-hydroxyethylmethacrylate

PGMEA

→

t-butylacrylate acrylic acid 2-hydroxyethylmethacrylate

반응 조건

후처리

1. 1
   기타were then polymerized at 60° C. for 8 hours
2. 2
   기타After completion of the polymerization
3. 3
   기타the mixture was precipitated in ether
4. 4
   여과filtered
5. 5
   기타dried in vacuo

실험 절차

12 g of t-butylacrylate, 5 g of acrylic acid, 3 g of 2-hydroxyethylmethacrylate and 0.4 g of AIBN were added to 200 g of PGMEA, and were then polymerized at 60° C. for 8 hours. After completion of the polymerization, the mixture was precipitated in ether, filtered, and dried in vacuo to yield 16 g of t-butylacrylate-acrylic acid-2-hydroxyethylmethacrylate copolymer, as a white solid, represented by Formula 2 below:

출처