반응 #2139927

반응 방정식

p-cyclohexylphenol

2-chloroethyl vinyl ether

sodium hydroxide

triethylamine

→

4-cyclohexylphenoxyethyl vinyl ether

용매

toluene

반응 조건

후처리

1. 1
   기타the mixture was reacted at 120° C. for 5 hours
2. 2
   세척The reaction solution was washed with water
3. 3
   workup.DISTILLATIONthe excessive 2-chloroethyl vinyl ether and toluene were distilled off
4. 4
   workup.DISTILLATIONthe resulting oil was purified by distillation in vacuo

실험 절차

In 300 ml of toluene, 83.1 g (0.5 moles) of p-cyclohexylphenol was dissolved, to which were then added 150 g of 2-chloroethyl vinyl ether, 25 g of sodium hydroxide, 5 g of tetrabutylammonium bromide and 60 g of triethylamine, and the mixture was reacted at 120° C. for 5 hours. The reaction solution was washed with water, the excessive 2-chloroethyl vinyl ether and toluene were distilled off, and the resulting oil was purified by distillation in vacuo to obtain 4-cyclohexylphenoxyethyl vinyl ether.

출처