반응 #2139926

ord-30ba1818977d4670a24a24a0170e33ea

반응 방정식

C=COCC
Ethyl vinyl ether
OCc1ccccc1
benzyl alcohol
C=COCc1ccccc1
benzyl vinyl ether

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    추출The reaction mixture was extracted with ethyl acetate
  2. 2
    추출the ethyl acetate extract
  3. 3
    세척was washed with water
  4. 4
    workup.DISTILLATIONfollowed by distillation in vacuo

실험 절차

Ethyl vinyl ether was mixed in benzyl alcohol, to which was then added mercury acetate, and the mixture was stirred at room temperature for 12 hours. The reaction mixture was extracted with ethyl acetate and the ethyl acetate extract was washed with water, followed by distillation in vacuo to obtain benzyl vinyl ether.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07326513B2uspto-grants-2008_02