반응 #2133
ord-465ca427a226420c828105b026a9c1d8
반응 방정식
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타chromatographed on silica gel (eluent: dichloromethane/methanol 20:1)
실험 절차
The title substance was prepared from 0.015 mol of diethyl [3-(3-methyl-xanthin-1-yl)propyl]phosphonate (Example 42), and 0.017 mol of chloromethylcyclopropane analogously to Example 30 and chromatographed on silica gel (eluent: dichloromethane/methanol 20:1).