반응 #2125

반응 방정식

3-ethylxanthine

benzyl bromide

potassium carbonate

→

7-Benzyl-3-ethylxanthine

용매

water

반응 조건

후처리

1. 1
   여과The precipitate was filtered off with suction
2. 2
   세척washed several times with warm water
3. 3
   기타dried at 50° C. under reduced pressure

실험 절차

18 g (0.1 mol) of 3-ethylxanthine were stirred at 60° C. for 2 hours with 19.2 g (0.11 mol) of benzyl bromide and 15.2 g (0.11 mol) of potassium carbonate. The reaction solution was transferred to an Edenmeyer flask and treated with 1000 ml of water. The precipitate was filtered off with suction, washed several times with warm water and dried at 50° C. under reduced pressure.

출처