반응 #2108

반응 방정식

5-(diethylphosphono)pentyl acetate

sodium carbonate

→

Diethyl 5-hydroxypentylphosphonate

용매

methanol

반응 조건

후처리

1. 1
   여과The solution was filtered
2. 2
   농축concentrated
3. 3
   workup.DISTILLATIONdistilled in a bulb tube

실험 절차

92 g (0.345 mol) of 5-(diethylphosphono)pentyl acetate were heated at 50° C. for 10 hours with stirring with 74 g (0.7 mol) of finely powdered sodium carbonate in 500 ml of methanol. The solution was filtered, concentrated and distilled in a bulb tube.

출처