반응 #2075714

ord-9a9f0a1470984ce2842aab81852b12a4

반응 방정식

ClOCl.[Zr]
zirconium oxychloride
O=S(=O)([O-])[O-].[Na+].[Na+]
sodium sulfate
Cl
hydrochloric acid
→
O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Zr+4]
zirconium sulfate

반응물

ClOCl.[Zr]
zirconium oxychloride
O=S(=O)([O-])[O-].[Na+].[Na+]
sodium sulfate
Cl
hydrochloric acid

시약

없음

반응 조건

온도
75°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    온도maintained for 1 hour to age

실험 절차

625 g of a 16% (ZrO2 conversion) zirconium oxychloride solution at room temperature was added to 237 g of a 25% sodium sulfate solution. After addition of hydrochloric acid to achieve a free acid concentration of 1.5 N, this was heated to 75° C. and maintained for 1 hour to age while producing basic zirconium sulfate.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07642210B2uspto-grants-2010_01