반응 #2075712

ord-3992c91f44c94de8a319155445453082

반응 방정식

O=S(=O)([O-])[O-].[Na+].[Na+]
sodium sulfate
ClOCl.[Zr]
zirconium oxychloride
Cl
hydrochloric acid
O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Zr+4]
zirconium sulfate

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.ADDITIONwas added
  2. 2
    온도this was maintained for 0.5 hours

실험 절차

94 g of a 25% sodium sulfate solution was heated to 65° C., 250 g of a 16% (by ZrO2 conversion) zirconium oxychloride solution which had been previously heated to 75° C. was added thereto, hydrochloric acid was added to achieve a free acid concentration of 1.5 N and this was maintained for 0.5 hours to produce basic zirconium sulfate (low-temperature reaction liquid).

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07642210B2uspto-grants-2010_01