반응 #2075712
ord-3992c91f44c94de8a319155445453082
반응 방정식
sodium sulfate
zirconium oxychloride
hydrochloric acid
→
zirconium sulfate
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.ADDITIONwas added
- 2온도this was maintained for 0.5 hours
실험 절차
94 g of a 25% sodium sulfate solution was heated to 65° C., 250 g of a 16% (by ZrO2 conversion) zirconium oxychloride solution which had been previously heated to 75° C. was added thereto, hydrochloric acid was added to achieve a free acid concentration of 1.5 N and this was maintained for 0.5 hours to produce basic zirconium sulfate (low-temperature reaction liquid).