반응 #2069941

반응 방정식

Thionyl chloride

4-n-butylbenzyl alcohol

→

title compound

수율 104.9%

1-(Chloromethyl)-4-n-butylbenzene

수율 104.9%

용매

ether

반응 조건

후처리

1. 1
   기타After concentration of the mixture, excess thionyl chloride was removed by azeotropic distillation with benzene

실험 절차

Thionyl chloride (2.5 ml, 34 mmol) was added to a solution of 4-n-butylbenzyl alcohol (2.0 g, 12 mmol) in ether (25 ml), and this mixture was stirred at room temperature for 3 hours. After concentration of the mixture, excess thionyl chloride was removed by azeotropic distillation with benzene to give the title compound (2.3 g). This compound was used in the following reaction without purification.

출처