반응 #2063069

ord-e03ce964b4e44eaca1fbdce626526773

반응 방정식

[Na+].[OH-]
sodium hydroxide
CCCCCCCCCCCCCCCCCCCCCC(=O)O
behenic acid
CCCCCCCCCCCCCCCCCCCC(=O)O
arachidic acid
CCCCCCCCCCCCCCCCCC(=O)O
stearic acid
O=[N+]([O-])O
nitric acid
CCCCCCCCCCCCCCCCCCCCCC(=O)[O-].[Na+]
sodium behenate

용매

반응 조건

온도
55°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.STIRRINGwith stirring for a period of 30 min.

실험 절차

In 945 ml of water were dissolved 32.4 g of behenic acid, 9.9 g of arachidic acid and 5.6 g of stearic acid at 90° C. Thereafter, an aqueous 1.5M sodium hydroxide solution was added with stirring at a high speed. Subsequently, 0.93 ml of concentrated nitric acid was added thereto and cooled 55° C. with stirring for a period of 30 min. to obtain a sodium behenate solution.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US06224988B1uspto-grants-2001_05