반응 #2063053

반응 방정식

2,3,3-trimethylindolenine

1,3-diiodopropane

→

1-[3-iodopropyl]-2,3,3-trimethyl-3H-indolium iodide

반응 조건

후처리

1. 1
   기타The resulting solid is recrystallized from ethanol

실험 절차

To a 50 mL round bottom flask is added 2,3,3-trimethylindolenine (14.4 mmol) and 1,3-diiodopropane (72.7 mmol) and the mixture is stirred at 60° C. under an atmosphere of nitrogen for 16 hours. The resulting solid is recrystallized from ethanol to give 1-[3-iodopropyl]-2,3,3-trimethyl-3H-indolium iodide (40) as crystals.

출처