반응 #2028868

반응 방정식

Methyl iodide

potassium carbonate

o-thiocresol

hexane

→

desired material

2-methylthioanisole

용매

DMF

water

반응 조건

후처리

1. 1
   기타The organic layer was separated
2. 2
   건조dried over magnesium sulfate
3. 3
   농축concentrated

실험 절차

Methyl iodide (0.5 mL, 8.1 mmol) and potassium carbonate (1.1 g, 8.1 mmol) were added to a solution of o-thiocresol (1.0 g, 8.1 mmol) in 10 mL of DMF. The reaction was stirred at 50° C., for 4 hours and poured into hexane and water. The organic layer was separated, dried over magnesium sulfate and concentrated to afford 1.1 g of desired material.

출처