반응 #2021473

반응 방정식

perfluorooctanesulfonic acid

silver carbonate

→

silver perfluorooctanesulfonate

용매

water

반응 조건

후처리

1. 1
   workup.ADDITIONwas added
2. 2
   workup.STIRRINGAfter stirring at room temperature for 3 days
3. 3
   여과the mixture was filtered
4. 4
   여과the obtained filter-cake
5. 5
   세척was washed with 10 parts of ion-exchange water
6. 6
   건조20 parts of diethylether and dried

실험 절차

Into a four-necked flask were charged 75 parts of perfluorooctanesulfonic acid and 100 parts of water, and 21.4 parts of silver carbonate was added thereto with stirring. After stirring at room temperature for 3 days, the mixture was filtered and the obtained filter-cake was washed with 10 parts of ion-exchange water, then 20 parts of diethylether and dried to give 60.3 parts of silver perfluorooctanesulfonate.

출처