반응 #1991766

반응 방정식

product

α-[(acetylthio)-methyl]-N-(hexahydro-1H-azepinyl)-benzene propanamide

sodium hydroxide

→

expected product

수율 97.2%

N-(hexahydro-1H-azepinyl)-α-(mercaptomethyl)-benzene propanamide

수율 97.2%

반응 조건

후처리

1. 1
   기타were reacted

실험 절차

Using the procedure of Example 6, 2 g of the product of Example 7 and 62.8 ml of 0.1N sodium hydroxide were reacted to obtain after chromatography on silica (eluent:methylene chloride - methanol, 100-2), 1.7 g of the expected product melting at about 82° C.

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