반응 #1925213

반응 방정식

methyl acrylate

diethanolamine

→

N,N-bis(2-hydroxyethyl)-2-(methoxycarbonyl)ethylamine

수율 98.0%

반응 조건

후처리

1. 1
   농축The reaction mixture was concentrated under reduced pressure

실험 절차

At 20 to 30° C., 9.01 g of methyl acrylate was added to 10.0 g of diethanolamine. The resulting mixture was allowed to stand for 20 hours. The reaction mixture was concentrated under reduced pressure, whereby N,N-bis(2-hydroxyethyl)-2-(methoxycarbonyl)ethylamine was obtained (yield: 98%).

출처