반응 #1914811

반응 방정식

3-methyl-1,4-benzoquinone-4-oxime

acetic anhydride

→

3-methyl-1,4-benzoquinone-4-(O-acetyloxime)

용매

반응 조건

후처리

1. 1
   기타At the end of the reaction
2. 2
   여과The precipitated product was filtered off
3. 3
   세척washed with water
4. 4
   기타dried

실험 절차

One drop of pyridine was added to a mixture of 0.5 g (3.6 mmol) of 3-methyl-1,4-benzoquinone-4-oxime and 1 mL of acetic anhydride and the resulting mixture was heated to 70° C. At the end of the reaction, the reaction mixture was poured on 10 mL of water/ice. The precipitated product was filtered off, washed with water and then dried.

출처