반응 #1904041

ord-5e11c941b17046ef94b03835ee80a6cd

반응 방정식

Oc1ccc(Br)cc1
p-bromophenol
BrCc1ccccc1
benzyl bromide
Brc1ccc(OCc2ccccc2)cc1
4-benzyloxybromobenzene

용매

반응 조건

온도
80°CELSIUS
상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.ADDITIONwere added

실험 절차

To a solution composed of p-bromophenol (17.3 g, 0.1 mol) and dry DMF (100 mL), anhydride K2CO3 (8.28 g, 0.06 mmol) and benzyl bromide (25.6 g, 0.15 mmol) were added. The mixture was stirred at 80° C. under a nitrogen atmosphere for six hours. Then, the reaction mixture was charged into 500 mL of ice water.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07597980B2uspto-grants-2009_10