반응 #1904041
ord-5e11c941b17046ef94b03835ee80a6cd
반응 방정식
p-bromophenol
benzyl bromide
→
4-benzyloxybromobenzene
용매
반응 조건
온도
80°CELSIUS
상세 조건
See reaction.notes.procedure_details.
후처리
- 1workup.ADDITIONwere added
실험 절차
To a solution composed of p-bromophenol (17.3 g, 0.1 mol) and dry DMF (100 mL), anhydride K2CO3 (8.28 g, 0.06 mmol) and benzyl bromide (25.6 g, 0.15 mmol) were added. The mixture was stirred at 80° C. under a nitrogen atmosphere for six hours. Then, the reaction mixture was charged into 500 mL of ice water.