반응 #1904039

반응 방정식

hydroxy amine

glutaric anhydride

→

Hydroxylamine Glutarate

용매

benzene

triethyl amine

반응 조건

후처리

1. 1
   온도refluxed for 2 h
2. 2
   기타The solvent is evaporated under vacuum
3. 3
   기타the residue is purified by flash chromatography

실험 절차

This example that demonstrates how this method could be performed. Part 1: To a solution of 2 g hydroxy amine in 100 ml dry benzene and 20 ml triethyl amine, 9.4 g glutaric anhydride is added and the reaction mixture stirred at room temperature for 2 h and refluxed for 2 h. The solvent is evaporated under vacuum and the residue is purified by flash chromatography using silica gel.

출처