반응 #1891307

반응 방정식

4-bromo-2-(1,1-dioxoisothiazolidin-2-yl)benzoic acid

1-(5-ethyl-3-methylpyridin-2-yl)piperazine

→

title compound

수율 94.1%

[4-bromo-2-(1,1-dioxoisothiazolidin-2-yl)phenyl][4-(5-ethyl-3-methylpyridin-2-yl)piperazin-1-yl]methanone

수율 94.1%

반응 조건

후처리

1. 1
   기타By reaction and treatment in the same manner
2. 2
   기타as in Preparation Example 90
3. 3
   기타described in Preparation Example 53

실험 절차

By reaction and treatment in the same manner as in Preparation Example 90 and using 4-bromo-2-(1,1-dioxoisothiazolidin-2-yl)benzoic acid (4.80 g) described in Preparation Example 178 and 1-(5-ethyl-3-methylpyridin-2-yl)piperazine (3.08 g) described in Preparation Example 53, the title compound (7.16 g) was obtained.

출처