반응 #1876820

반응 방정식

1,3,5-trihydroxyadamantane

trimethylamine

trimethylsilyl chloride

→

1,3-dihydroxy-5-trimethylsiloxyadamantane

용매

methylene chloride

반응 조건

후처리

1. 1
   기타Reaction
2. 2
   기타was carried out at room temperature
3. 3
   기타The reaction product was partitioned by high performance liquid chromatography

실험 절차

This 1,3,5-trihydroxyadamantane was dissolved in methylene chloride. To this solution were added a small amount of trimethylamine, and then an equimolar amount of trimethylsilyl chloride. Reaction was carried out at room temperature. The reaction product was partitioned by high performance liquid chromatography to obtain 1,3-dihydroxy-5-trimethylsiloxyadamantane.

출처