반응 #1869202

반응 방정식

1,1-dimethylethyl {1-[2-(4-quinolinyl)ethyl]-4-piperidinyl}carbamate

chloroform

→

product

수율 100.0%

1-[2-(4-quinolinyl)ethyl]-4-piperidinamine trihydrochloride

수율 100.0%

용매

HCl

dioxane

반응 조건

후처리

1. 1
   기타the reaction mixture was evaporated to dryness

실험 절차

1,1-dimethylethyl {1-[2-(4-quinolinyl)ethyl]-4-piperidinyl}carbamate (9a) (278 mg) was dissolved in chloroform and diluted with 4N HCl in dioxane solution. After stirring two hours, the reaction mixture was evaporated to dryness to afford the product as a solid (180 mg, 100%).

출처