반응 #1862608

반응 방정식

3-(phenylsulfenyl)-2-iodobenzo[b]thiophene

3-(phenylselenenyl)-2-iodobenzo[b]thiophene

→

[1]benzoselenopheno[3,2-b][1]benzothiophene

수율 85.0%

반응 조건

후처리

1. 1
   기타Purification
2. 2
   기타was produced (yield: 85%)

실험 절차

Except that 3-(phenylsulfenyl)-2-iodobenzo[b]thiophene was replaced with 3-(phenylselenenyl)-2-iodobenzo[b]thiophene, the reaction was implemented in the same way as in Example 3. Purification was implemented by column chromatography (silica gel, CHCl3, Rf: 0.9), so that a yellow solid was produced (yield: 85%).

출처