반응 #1858813

반응 방정식

2,6-dimethylaniline

acetic anhydride

→

title compound

수율 74.0%

N-(2,6-dimethylphenyl)acetamide

수율 74.0%

반응 조건

후처리

1. 1
   기타the precipitate that formed
2. 2
   여과collected by filtration

실험 절차

2,6-dimethylaniline (10 g, 82.5 mmol, 1.0 eq) was added to acetic anhydride (100 mL) at 0° C. The reaction mixture was then warmed to room temperature and stirred for 1 h. The reaction was poured into ice water and the precipitate that formed collected by filtration to give the title compound as a yellow solid (10 g, 74%).

출처