반응 #1857539

ord-628b2d626b2d4d7b8566dd0f610afc84

반응 방정식

Cc1ccccc1
toluene
CCC(C)=O
methyl ethyl ketone
CCCCCCCCCCCC(=O)OCC(O)CO
Lauricidin
CCCCCCCCCCCC(=O)OCC(O)CO
Lauricidin
수율 20.0%
O=C(O)c1ccccc1O
salicylic acid
수율 10.0%

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    workup.DISSOLUTIONwas dissolved
  2. 2
    기타gave 100% microbial load reduction for gram positive pathogens and 99.4% microbial load reduction for gram negative pathogens

실험 절차

A fluid solution of 20.0% Lauricidin, 10.0% salicylic acid, and 10.0% DOSS surfactant in isopropanol was prepared by stirring the mixture until the Lauricidin was dissolved. 20% of the fluid solution was combined with 80% of the hardcoat mixture described in Examples 1-11 (i.e., 100 parts of 3M 906 Hardcoat with 12 parts toluene and 12 parts methyl ethyl ketone). The combined solution was coated and cured as described in Examples 1-11. The resulting multi-layer film was clear and transparent. The resulting multi-layer film was then tested for microbial load reduction, as described above in Examples 1-11, and gave 100% microbial load reduction for gram positive pathogens and 99.4% microbial load reduction for gram negative pathogens.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US09247736B2uspto-grants-2016_02