반응 #1821006
ord-61663a4397574c57a3f2de0a8e71935c
반응 방정식
sodium
chloromethylcarbonylmethylenetriphenyl phosphorane
isopropoxymethylcarbonylmethylenetriphenyl phosphorane
→
title compound
(2-Isopropoxyethyl)-carbonylmethylenetriphenyl phosphorane
반응물
시약
없음
반응 조건
상세 조건
See reaction.notes.procedure_details.
실험 절차
A solution of 3.04 g of sodium in 100 ml of 3-pentanol is reacted with 25.0 g of chloromethylcarbonylmethylenetriphenyl phosphorane analogously to the production of isopropoxymethylcarbonylmethylenetriphenyl phosphorane. The title compound is obtained as crystallized oil with a melting point of 66°-70° C.