반응 #1820221
ord-389aae5f606d4c48b936d86f9a8ec6ac
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과The catalyst is filtered off
- 2기타the solution is evaporated
실험 절차
A solution of 2.77 g of 1-pyrrolidino-3-p-biphenylyl-1-butene (obtainable from 3-p-biphenylyl-butanal and pyrrolidine) in 35 ml of ethanol is hydrogenated over 0.5 g of Raney nickel, for 3 hours at 6 atms and 60°. The catalyst is filtered off and the solution is evaporated to give 1-pyrrolidino-3-p-biphenylyl-butane.