반응 #1820221

ord-389aae5f606d4c48b936d86f9a8ec6ac

용매

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    여과The catalyst is filtered off
  2. 2
    기타the solution is evaporated

실험 절차

A solution of 2.77 g of 1-pyrrolidino-3-p-biphenylyl-1-butene (obtainable from 3-p-biphenylyl-butanal and pyrrolidine) in 35 ml of ethanol is hydrogenated over 0.5 g of Raney nickel, for 3 hours at 6 atms and 60°. The catalyst is filtered off and the solution is evaporated to give 1-pyrrolidino-3-p-biphenylyl-butane.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US04239759uspto-grants-1980_12