반응 #1818824
ord-645e3c7bf23e44ca89ff93185df59085
반응 방정식
1-oxo2,3,9,10-tetrahydro-1H-benzo[b]indeno[5,4-f]thiepin-6-carboxylic acid
1-oxo2,3,11,12-tetrahydro-1H-benzo[b]indeno[4,5-f]thiepin-8-carboxylic acid
→
title compound
2,3,9,10-Tetrahydro-1H-benzo[b]indeno[5,4-f]thiepin-6-carboxylic acid
반응물
시약
없음
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1온도heating
- 2온도under reflux for 9 hours instead of 3 hours
실험 절차
Substituting an equivalent amount of 1-oxo2,3,9,10-tetrahydro-1H-benzo[b]indeno[5,4-f]thiepin-6-carboxylic acid in Example 41 in place of 1-oxo2,3,11,12-tetrahydro-1H-benzo[b]indeno[4,5-f]thiepin-8-carboxylic acid and heating under reflux for 9 hours instead of 3 hours yielded the title compound.