반응 #1797523

ord-fe5d8300618f438fb631db0038c40ea6

반응 방정식

O=C(NC1C2CC3CC(C2)CC1C3)c1cnn(-c2ccccc2)c1Cl
5-chloro-1-phenyl-1H-pyrazole-4-carboxylic acid adamantan-2-ylamide
O=C(NC1C2CC3CC(C2)CC1C3)c1cnn(-c2ccccc2)c1Cl
Intermediate 3
O=C(NC1C2CC3CC(C2)CC1C3)c1cnn(-c2ccccc2)c1Cl
5-chloro-1-phenyl-1H-pyrazole-4-carboxylic acid adamantan-2-ylamide
NCc1ccccc1
benzylamine
→
O=C(NC1C2CC3CC(C2)CC1C3)c1cnn(-c2ccccc2)c1NCc1ccccc1
5-Benzylamino-1-phenyl-1H-pyrazole-4-carboxylic acid adamantan-2-ylamide

반응물

O=C(NC1C2CC3CC(C2)CC1C3)c1cnn(-c2ccccc2)c1Cl
5-chloro-1-phenyl-1H-pyrazole-4-carboxylic acid adamantan-2-ylamide
O=C(NC1C2CC3CC(C2)CC1C3)c1cnn(-c2ccccc2)c1Cl
Intermediate 3
O=C(NC1C2CC3CC(C2)CC1C3)c1cnn(-c2ccccc2)c1Cl
5-chloro-1-phenyl-1H-pyrazole-4-carboxylic acid adamantan-2-ylamide
NCc1ccccc1
benzylamine

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

5-Benzylamino-1-phenyl-1H-pyrazole-4-carboxylic acid adamantan-2-ylamide was prepared using Procedure A from 5-chloro-1-phenyl-1H-pyrazole-4-carboxylic acid adamantan-2-ylamide (Intermediate 3) and benzylamine. Mass spectrum (ES) MH+=427.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US07790711B2uspto-grants-2010_09