반응 #1797481

반응 방정식

CF3OCF(CF3)CF2OCF═CF2

isopropanol

→

CF3OCF(CF3)CF2OCFHCF2C(CH3)2OH

반응 조건

후처리

1. 1
   기타at 75° C
2. 2
   기타The resulting product reaction mixture
3. 3
   workup.DISTILLATIONwas distilled
4. 4
   기타=161-166° C.

실험 절차

CF3OCF(CF3)CF2OCFHCF2C(CH3)2OH was prepared by the reaction of CF3OCF(CF3)CF2OCF═CF2 (52.9 g, 0.16 mol) with isopropanol (202 g, 3.37 mol) using LUPEROX 575 (11.4 g) as free radical initiator at 75° C. The resulting product reaction mixture was distilled and the distillation fraction of b.r.=161-166° C. used in the next step.

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