반응 #1797478
ord-49530173db4a46ca88018fc46e3407e0
반응 방정식
chlorpheniramine maleate
→
Chlorpheniramine
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1세척the product washed with USP water
- 2기타The wet cake was dried
- 3여과sieved through a US Std #30 mesh screen
실험 절차
Chlorpheniramine polistirex was prepared by mixing 3.12 kg of chlorpheniramine maleate with 26.00 kg of ion-exchange resin particles (AMBERLITE IRP69; US Std. Mesh #100-#400) suspended in USP water at about 30° C. The resulting suspension was centrifuged and the product washed with USP water. The wet cake was dried and sieved through a US Std #30 mesh screen. The chlorpheniramine content of the dried product was equivalent to approximately 11% by weight.