반응 #1796432
ord-09a92b4e87f24e9ba1561793d208ec81
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타in 2 hours
- 2기타at 15° to 20° C
- 3기타The solvent was removed by distillation under reduced pressure
실험 절차
10.9 g of ethyl (E)-3-(3-acetylphenyl)acrylate was dissolved in 50 ml of ethanol and 5 ml of dioxane. To the solution was dropwise added 8.8 g of bromine in 2 hours at 15° to 20° C. The mixture was stirred for 1 hour at the same temperature. The solvent was removed by distillation under reduced pressure to obtain ethyl (E)-3-[3-(2-bromoacetyl)phenyl]acrylate.