반응 #1771993
ord-40794a691015423f8f8e6dd4b847146a
반응 방정식
Boc-4-phenylproline
→
product
수율 95.4%
Boc-4-cyclohexylproline
수율 95.4%
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1여과The mixture was filtered
- 2농축concentrated
실험 절차
A solution of the commercially available Boc-4-phenylproline (750 mg) and 5% Rh on carbon (750 mg) in methanol (15 mL) was hydrogenated at 50 psi for 24 hours. The mixture was filtered and concentrated to give 730 mg of product.