반응 #1771990
ord-56238b79bf8e4876a8c816dff94dc2f6
반응 방정식
tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline
→
4,4-Dimethylproline
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1농축The solution was concentrated
- 2기타dried under high vacuum
- 3기타taken to the next step without further purification
실험 절차
A solution of tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline in dichloromethane (5 mL) and trifluoroacetic (5 mL) was stirred at room temperature for five hours. The solution was concentrated, dried under high vacuum and taken to the next step without further purification.