반응 #1771990

ord-56238b79bf8e4876a8c816dff94dc2f6

반응 방정식

CC1(C)CN(C(=O)OC(C)(C)C)[C@@](C(=O)O)(C(C)(C)C)C1
tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline
CC1(C)CN[C@H](C(=O)O)C1
4,4-Dimethylproline

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    농축The solution was concentrated
  2. 2
    기타dried under high vacuum
  3. 3
    기타taken to the next step without further purification

실험 절차

A solution of tert-butyl N-tert-butoxycarbonyl-4,4-dimethylproline in dichloromethane (5 mL) and trifluoroacetic (5 mL) was stirred at room temperature for five hours. The solution was concentrated, dried under high vacuum and taken to the next step without further purification.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: USRE043298E1uspto-grants-2012_04