반응 #1764048

반응 방정식

diethylmethylamine

p-toluenesulfonic acid monohydrate

→

diethylmethylamine

p-toluenesulfonic acid

용매

2-butanone

반응 조건

후처리

1. 1
   workup.DISTILLATIONthe solvent was then distilled off in vacuo
2. 2
   기타The obtained solid was recrystallized from acetone

실험 절차

3.0 g of diethylmethylamine was dissolved in 30 cm3 of 2-butanone, to which was then gradually added 5.7 g of p-toluenesulfonic acid monohydrate while stirring. The stirring was continued for an additional one hour, and the solvent was then distilled off in vacuo. The obtained solid was recrystallized from acetone to obtain a diethylmethylamine salt of p-toluenesulfonic acid.

출처