반응 #1755455

반응 방정식

1-(4′-phenylsulfonylphenyl)benzimidazole

trimethyloxonium tetrafluoroborate

ethanol

→

1-(4′-phenylsulfonylphenyl)-3-methylbenzimidazolium tetrafluoroborate

수율 80.0%

용매

dichloromethane

반응 조건

후처리

1. 1
   여과the precipitate which forms is filtered off
2. 2
   세척washed with cold petroleum ether

실험 절차

A solution of 1-(4′-phenylsulfonylphenyl)benzimidazole (6.7 g, 20 mmol) in dichloromethane (100 ml) is admixed at −10° C. with trimethyloxonium tetrafluoroborate (3.3 g, 22 mmol) and stirred under argon for 16 h. After adding ethanol, the precipitate which forms is filtered off and washed with cold petroleum ether. Yield: 80%.

출처