반응 #1748

ord-98aa976f41dc49e1bd5ec855777b801d

반응 방정식

CN(C)Cc1ccc([C@H]2CC[C@H](O)CC2)cc1
trans-4-(4-dimethylaminomethylphenyl)-cyclohexanol
CC(=O)Cl.CCN(CC)CC
acetylchloride triethylamine
→
CC(=O)O[C@H]1CC[C@H](c2ccc(CN(C)C)cc2)CC1
trans-O-acetyl-4-(4-dimethylaminomethylphenyl)-cyclohexanol

반응물

CN(C)Cc1ccc([C@H]2CC[C@H](O)CC2)cc1
trans-4-(4-dimethylaminomethylphenyl)-cyclohexanol
CC(=O)Cl.CCN(CC)CC
acetylchloride triethylamine

시약

없음

반응 조건

상세 조건
See reaction.notes.procedure_details.

실험 절차

from trans-4-(4-dimethylaminomethylphenyl)-cyclohexanol and acetylchloride/triethylamine. Colourless syrup.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US05726205uspto-grants-1998_03