반응 #1747852

반응 방정식

4-carboxyphenylthiourea

DIC

→

Phenylthiourea

용매

DMF

반응 조건

후처리

1. 1
   기타Aminopropylsilylated glass surfaces purified with compressed air (2.5×7.5 cm; Sigma, Silane-Prep™, S4651)
2. 2
   기타thus obtained
3. 3
   workup.ADDITIONThe glass surfaces thus treated
4. 4
   세척were then washed five times
5. 5
   기타for 3 minutes
6. 6
   기타at room temperature
7. 7
   세척After washing three times for three minutes each using respectively 30 mL of DCM at room temperature
8. 8
   기타the glass surfaces were dried
9. 9
   기타stored at 4° C. until further use

실험 절차

4-carboxyphenylthiourea (Lancaster, 13047) was dissolved to 0.2M in DMF. The resultant mixture was activated by adding a half equivalent of DIC for 15 min at room temperature. Aminopropylsilylated glass surfaces purified with compressed air (2.5×7.5 cm; Sigma, Silane-Prep™, S4651) were coated with the activated solution thus obtained and incubated for three hours at room temperature. The glass surfaces thus treated were then washed five times using respectively 30 mL of DMF for 3 minutes each at room temperature. After washing three times for three minutes each using respectively 30 mL of DCM at room temperature, the glass surfaces were dried and stored at 4° C. until further use.

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