반응 #1744950

ord-234b282704d9437bb72aec82c45e6e27

반응 방정식

Cc1ccccc1CCCN1C[C@@H](C)NC[C@@H]1C
trans-1-[3-(o-methylphenyl)propyl]-2,5-dimethylpiperazine
O=C(Cl)c1ccco1
2-furoyl chloride
→
Cc1ccccc1CCCN1C[C@@H](C)N(C(=O)c2ccco2)C[C@@H]1C.Cl
trans-1-[3-(o-Methylphenyl)propyl]-2,5-dimethyl-4-(2-furoyl)piperazine hydrochloride

반응물

Cc1ccccc1CCCN1C[C@@H](C)NC[C@@H]1C
trans-1-[3-(o-methylphenyl)propyl]-2,5-dimethylpiperazine
O=C(Cl)c1ccco1
2-furoyl chloride

시약

없음

용매

c1ccccc1
benzene

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The compound was obtained

실험 절차

The compound was obtained by following the same process as in Example 2 from a mixture of trans-1-[3-(o-methylphenyl)propyl]-2,5-dimethylpiperazine [b.p. 130° - 140°C (4 mmHg), dipicrate, 250° - 252°C], 2-furoyl chloride and benzene.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US03962249uspto-grants-1976_06