반응 #1708380
ord-d9fd6f8899674acb8d20ae54423b0202
시약
없음
용매
반응 조건
상세 조건
See reaction.notes.procedure_details.
후처리
- 1기타Slowly add hydrochloric acid, and white precipitation
- 2workup.STIRRINGStir the slurry for at least 4 hours
- 3여과filter the slurry
실험 절차
In a large beaker, add naphthionic acid sodium salt and water and stir to complete solution, pH=9.2-9.4. Slowly add hydrochloric acid, and white precipitation occurs at pH=2.2-2.4. Stir the slurry for at least 4 hours, then filter the slurry. Use the wetcake in Stage 2.