반응 #1702112

반응 방정식

2-(3-nitrophenyl)ethanol

→

desired product

수율 99.0%

2-(3-Aminophenyl)ethanol

수율 99.0%

용매

methanol

반응 조건

후처리

1. 1
   기타was hydrogenated at 45 psi overnight
2. 2
   여과The resultant mixture was filtered
3. 3
   농축concentrated

실험 절차

Into a pressure bottle were added 2-(3-nitrophenyl)ethanol (3.0 g, 18 mmol) and methanol (100 mL) and 10% palladium on carbon (0.1 g, 0.08 mmol). The reaction mixture was hydrogenated at 45 psi overnight. The resultant mixture was filtered and concentrated to provide the desired product (2.44 g, 99%) as a white solid. LCMS for C8H12NO (M+H)+: m/z=138.1.

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