반응 #1702020

반응 방정식

Ethylidenenorbornene

Butyl ether

diethylaluminumchloride

→

Dicyclopentadiene Ethylidenenorbornene

용매

dicyclopentadiene

반응 조건

후처리

1. 1
   기타was then capped with a septum
2. 2
   기타purged with nitrogen
3. 3
   workup.DISSOLUTIONto dissolve the solids

실험 절차

Irganox™ 1010 (0.24 g, Ciba Specialty Chemical Corp, Tarrytown, N.Y.) and Irgafos™ 168 (0.72 g, Ciba) were placed in an oven-dried 125 mL Erlenmeyer flask which was then capped with a septum and purged with nitrogen. Ethylidenenorbornene (35.6 mL, 0.26 mol) was added and the mixture was stirred for several minutes to dissolve the solids. Butyl ether (2.4 mL) and 9.1 mL of a 10 vol % solution of diethylaluminumchloride in dicyclopentadiene were then added. This solution is denoted Mixture 4B.

출처