반응 #169353

ord-71b6755b6b1c429897d3d2f5d74f5487

반응 방정식

FC(F)(F)c1cn[nH]c1
4-(trifluoromethyl)-1H-pyrazole
CC(C)(C)OC(=O)CBr
tert butyl bromoacetate
CC(C)(C)OC(=O)Cn1cc(C(F)(F)F)cn1
title compound
CC(C)(C)OC(=O)Cn1cc(C(F)(F)F)cn1
tert-Butyl[4-(trifluoromethyl)-1H-pyrazol-1-yl]acetate

반응 조건

상세 조건
See reaction.notes.procedure_details.

후처리

  1. 1
    기타The title compound was prepared

실험 절차

The title compound was prepared according to the method described for Preparation 79 using 4-(trifluoromethyl)-1H-pyrazole and tert butyl bromoacetate to afford the title compound as a yellow solid in 24% yield, 1.32 g.

출처

DOI: 10.6084/m9.figshare.5104873.v1특허: US08846698B2uspto-grants-2014_09