반응 #1693407

반응 방정식

complex

ethyltoluene

phthalic anhydride

→

o-(p-toluyl)-benzoic acid

수율 107.5%

용매

toluene

반응 조건

후처리

1. 1
   workup.ADDITIONafter the addition
2. 2
   workup.ADDITIONThe reaction mixture was treated as usual

실험 절차

To a mixture of 108 g of the complex obtained in Example 1 and 92 g of toluene were added gradually 14.8 g of phthalic anhydride while stirring, and the mixture was maintained at 70°C for 2 hours after the addition. The reaction mixture was treated as usual to obtain 22.8 g of o-(p-toluyl)-benzoic acid.

출처